Glossary entry (derived from question below)
English term
at reflux
Does it mean stirring with making a tide? i.e clockwise and anticlockwise
4 +8 | at reflux | K Donnelly |
Oct 21, 2010 07:39: K Donnelly Created KOG entry
Non-PRO (1): Dr. Andrew Frankland
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Responses
at reflux
A liquid reaction mixture is placed in a vessel open only at the top. This vessel is connected to a Liebig or Vigreux condenser, such that any vapours given off are cooled back to liquid, and fall back into the reaction vessel. The vessel is then heated vigorously for the course of the reaction. The purpose is to thermally accelerate the reaction by conducting it at an elevated temperature (i.e. the solvent's boiling point).
http://en.wikipedia.org/wiki/Reflux
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