Glossary entry

English term or phrase:

at reflux

English answer:

at reflux

Added to glossary by K Donnelly
Oct 14, 2010 09:50
13 yrs ago
5 viewers *
English term

at reflux

English Law/Patents Chemistry; Chem Sci/Eng pharmaceutical
The reaction mixture was stirred at reflux for 3 h.
Does it mean stirring with making a tide? i.e clockwise and anticlockwise
Responses
4 +8 at reflux
Change log

Oct 21, 2010 07:39: K Donnelly Created KOG entry

Votes to reclassify question as PRO/non-PRO:

Non-PRO (1): Dr. Andrew Frankland

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Responses

+8
5 mins
Selected

at reflux

This is a common laboratory technique

A liquid reaction mixture is placed in a vessel open only at the top. This vessel is connected to a Liebig or Vigreux condenser, such that any vapours given off are cooled back to liquid, and fall back into the reaction vessel. The vessel is then heated vigorously for the course of the reaction. The purpose is to thermally accelerate the reaction by conducting it at an elevated temperature (i.e. the solvent's boiling point).

http://en.wikipedia.org/wiki/Reflux
Peer comment(s):

agree Dr. Andrew Frankland : Although I would tend to say "under reflux" rather than "at reflux".
18 mins
Thanks!
agree Thayenga : "under", yes.
57 mins
Thanks!
agree Karen Tkaczyk : I use both 'under' and 'at'. Both are fine.
3 hrs
Than you!
agree kamilw : both
4 hrs
Thank you!
agree Polangmar
1 day 6 hrs
Thanks!
agree Stephanie Ezrol
2 days 1 hr
Thanks!
agree Helen Genevier
2 days 3 hrs
Thank you!
agree CHEN-Ling
2 days 17 hrs
Thank you!
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4 KudoZ points awarded for this answer. Comment: "Thank you"
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